Pharma Case Studies

Proven compliance and engineering solutions executed across leading pharmaceutical plants in Egypt.

Validation & Qualification

Cleanroom & HVAC Qualification (Aseptic Filling Line)

10th of Ramadan City, Egypt

The Challenge

A prominent manufacturer of sterile injectables needed to qualify their Class A (ISO 5) aseptic filling room and its dedicated HVAC system to comply with the updated EU GMP Annex 1 guidelines. The plant faced strict deadlines for an upcoming regulatory inspection.

Our Solution

QEEMA's validation engineers executed a comprehensive qualification protocol. This included cleanroom air balancing, airborne particle count monitoring, HEPA filter integrity leak tests (DOP method), cleanroom pressure differential tests, recovery time determination, and smoke flow visualization (airflow pattern videos).

The Outcome

The facility successfully demonstrated compliance with EU GMP Annex 1 standards. Complete IQ/OQ/PQ documentation was generated and approved by the regulatory authority on the first audit, permitting immediate commercial sterile manufacturing.

Startup Projects

Validation Master Plan & Full Equipment IQ/OQ/PQ

Badr City, Egypt

The Challenge

A newly built solid-dosage pharmaceutical facility required a complete Validation Master Plan (VMP) and qualifications for all production equipment (high-shear mixers, fluid-bed dryers, tableting presses, and blister packaging machines) for their local EDA license inspection.

Our Solution

QEEMA designed a risk-based Validation Master Plan incorporating Quality Risk Management (QRM) principles. We drafted, executed, and archived individual IQ, OQ, and PQ protocols for every machine. We also performed cleaning validation limits calculations based on toxicological PDE data.

The Outcome

The EDA inspection team approved the VMP and validation records without any major or critical deficiencies. The plant received its commercial production license on schedule.

Thermal Mapping

WHO TRS 961 Thermal Mapping of 5,000 sqm Warehouse

Obour City, Egypt

The Challenge

A regional pharmaceutical distributor needed to perform thermal mapping of their 5,000 sqm high-rack warehouse to satisfy Good Distribution Practice (GDP) guidelines and WHO TRS 961 guidelines. They needed mapping for both summer and winter extremes.

Our Solution

QEEMA placed 45 pre-calibrated temperature and relative humidity loggers across three dimensions (bottom, middle, top levels) of the storage racks. The loggers collected data continuously for 7 days. We generated hot and cold spot profiles and calculated the Mean Kinetic Temperature (MKT).

The Outcome

Identified three hot spots near the high skylights and recommended localized ventilation tweaks. The mapping study complied fully with GDP audits, ensuring safe distribution of temperature-sensitive vaccines and biological drugs.